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Beiträge zur strukturchemischen Untersuchung von Wasserstoffbrückenbindungen in ammoniakhaltigen Aziden, Amiden und Ammoniumsalzen

URN to cite this document: urn:nbn:de:bvb:355-opus-13083

Scheubeck, Thomas Josef (2009) Beiträge zur strukturchemischen Untersuchung von Wasserstoffbrückenbindungen in ammoniakhaltigen Aziden, Amiden und Ammoniumsalzen. PhD, Universität Regensburg

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Abstract (German)

Im Rahmen dieser Arbeit wurden aus flüssigem Ammoniak folgende Verbindungen isoliert und strukturchemisch charakterisiert:
Rubidiumamid-Ammoniakat (3/2)
Natriumazid-Ammoniakat (1/5)
Kalium(18-krone-6)azid-Ammoniakat (1/1)
Rubidium(18-krone-6)azid-Ammoniakat (1/3)
Hexaamminkupfer(II)-azid-Ammoniakat (1/4)
Hexaamminnickel(II)-azid-Ammoniakat (1/4)
Hexaammincobalt(II)-azid-Ammoniakat (1/4)
Hexaammincadmium(II)-azid-Ammoniakat (1/4)
Hexaamminkupfer(II)-dicyanamid-Ammoniakat (1/2)
Hexaammincadmium(II)-dicyanamid-Ammoniakat (1/2)
Bis(ammonium)acetylendicarboxylat-Ammoniakat (1/6)
Ammoniumpentanoat-Ammoniakat (1/1)
Ammoniumhexanoat-Ammoniakat (1/1)
Ammoniumbenzoat-Ammoniakat (1/3)
Ammoniumphthalat-Ammoniakat (1/2)
Ammoniumisophthalat-Ammoniakat (1/6)
Ammoniumterephthalat- Ammoniakat (1/4)
Dabei wurden die enthaltenen Wasserstoffbrückenbindungen, insbesondere N-H...N-Wasserstoffbrückenbindungen statistisch erfasst und diskutiert.

Translation of the abstract (English)

Within this work, following compounds were isolated from liquid ammonia. Their structures were characterized by single crystal diffraction methods:
rubidium azide - ammonia (3/2)
sodium azide - ammonia (1/5)
potassium (18-crown-6) azide - ammonia (1/1)
rubidium (18-crown-6) azide - ammonia (1/3)
hexaammine copper(II) azide - ammonia (1/4)
hexaammine nickel(II) azide - ammonia (1/4)
hexaammine cobalt(II) azide - ammonia (1/4)
hexaammine cadmium(II) azide - ammonia (1/4)
hexaammine copper(II) dicyanamide - ammonia (1/2)
hexaammine cadmium(II) dicyanamide - ammonia (1/2)
bis(ammonium) acetylene dicarboxylate - ammonia (1/6)
ammonium pentanoate -ammonia (1/1)
ammonium hexanoate - ammonia (1/1)
ammonium benzoate - ammonia (1/3)
ammonium phthalate - ammonia (1/2)
ammonium isophthalate - ammonia (1/6)
ammonium terephthalate - ammonia (1/4)
Hydrogen bonds within this compounds were evaluated statistically and discussed, especially N-H...N hydrogen bonds.

Item Type:	Thesis of the University of Regensburg (PhD)
Referee:	Nikolaus (Prof. Dr.) Korber
Date of exam:	13 July 2009
Institutions:	Chemistry and Pharmacy > Institut für Anorganische Chemie > Arbeitskreis Prof. Dr. Nikolas Korber
Keywords:	Azide , Ammoniak , Amide , Ammoniumverbindungen , Wasserstoffbrückenbindung , Wasserstoffbrückenbindungen , Dicyanamide , hydrogen bonds , azides , ammonia , amides , ammonium compounds
Subjects:	500 Science > 540 Chemistry & allied sciences
Status:	Published
Refereed:	Yes, this version has been refereed
Created at the University of Regensburg:	Yes
Owner:	Universitätsbibliothek Regensburg
Deposited On:	18 Jan 2010 15:08
Last Modified:	24 Oct 2012 08:50
Item ID:	12314

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