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Reduction of benzylidene alkylamines with activated aluminum in alcoholic solution

Thies, Heinrich and Schönenberger, Helmut and Bauer, K. H. (1958) Reduction of benzylidene alkylamines with activated aluminum in alcoholic solution. Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft 291, pp. 373-375.

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Abstract

Dialkyldiphenylethylenediamines and benzylalkylamines were formed on reduction of benzylidenealkylamines with activated Al. Al foil (5.4 g.) and a little HgCl2. in 120 ml. EtOH warmed until H began to evolve, 0.1 mole Schiff base in 30 ml. C6H6 added, the mixt. heated 2 hrs. on the H2O bath, treated with 100 ml. C6H6 and 100 ml. 15% aq. NaOH, heated 15 min. more, 200 ml. H2O added, the mixt. ...

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Item Type:Article
Date:1958
Additional information (public):CAN 53:11596 10E Organic Chemistry: Benzene Derivatives 58496-40-5; 108263-68-9; 108263-69-0; 110938-27-7; 110939-19-0; 111586-41-5; 114910-46-2 (Derived from data in the 6th Collective Formula Index (1957-1961); 7025-95-8P; 7030-59-3P; 82165-21-7P; 94801-41-9P; 859438-22-5P; 1086223-97-3P; 1086233-33-1P; 1087400-07-4P; 1087401-40-8P; 1088227-83-1P; 1088227-91-1P; 1129271-40-4P Role: SPN (Synthetic preparation), PRP (Properties), PREP (Preparation) (Reduction of benzylidene alkylamines with activated aluminum in alcoholic solution); 7429-90-5 (Aluminum) (active, N-alkyl benzylidenimine redn. by); 102-97-6P (Benzylamine, N-isopropyl-); 103-49-1P (Dibenzylamine); 103-67-3P (Benzylamine, N-methyl-); 2032-33-9P (Benzylamine, N-propyl-); 2403-22-7P (Benzylamine, N-butyl-); 3647-71-0P (Phenethylamine, N-benzyl-); 4169-62-4P (Ethylenediamine, N,N'-dibutyl-1,2-diphenyl-); 4383-25-9P (Benzylamine, N-cyclohexyl-); 14321-27-8P (Benzylamine, N-ethyl-); 15018-21-0P (Ethylenediamine, N,N'-diethyl-1,2-diphenyl-); 22751-68-4P (Ethylenediamine, N,N'-dimethyl-1,2-diphenyl-); 22751-69-5P (Ethylenediamine, N,N'-dicyclohexyl-1,2-diphenyl-); 24431-19-4P (Ethylenediamine, N,N'-dibenzyl-1,2-diphenyl-); 55079-98-6P (Ethylenediamine, N,N'-diisopropyl-1,2-diphenyl-); 96504-88-0P (Ethylenediamine, N,N'-dibutyl-1,2-diphenyl-, dihydrochloride); 102599-97-3P (Ethylenediamine, 1,2-diphenyl-N,N'-dipropyl-); 103276-50-2P (Ethylenediamine, N,N'-diphenethyl-1,2-diphenyl-); 112247-77-5P (Ethylenediamine, N,N'-diisopropyl-1,2-diphenyl-, dihydrochloride); 112247-78-6P (Ethylenediamine, 1,2-diphenyl-N,N'-dipropyl-, dihydrochloride); 114159-65-8P (Ethylenediamine, N,N'-dicyclohexyl-1,2-diphenyl-, dihydrochloride); 115292-46-1P (Ethylenediamine, N,N'-dibenzyl-1,2-diphenyl-, dihydrochloride); 115294-01-4P (Ethylenediamine, N,N'-diphenethyl-1,2-diphenyl-, dihydrochloride); 131762-27-1P (Ethylenediamine, N,N'-diethyl-1,2-diphenyl-, dihydrochloride); 878794-82-2P (Ethylenediamine, N,N'-dimethyl-1,2-diphenyl-, dihydrochloride) Role: PREP (Preparation) (prepn. of); 622-29-7 (Methylamine, N-benzylidene-); 780-25-6 (Benzylamine, N-benzylidene-); 1077-18-5 (Butylamine, N-benzylidene-); 2211-66-7 (Cyclohexylamine, N-benzylidene-); 3240-95-7 (Phenethylamine, N-benzylidene-); 6852-54-6 (Ethylamine, N-benzylidene-); 6852-55-7 (Propylamine, N-benzylidene-); 6852-56-8 (Ethylamine, N-benzylidene-1-methyl-) (redn. of)
Institutions:Chemistry and Pharmacy > Institute of Pharmacy > Retired Professors > Prof. Schönenberger
Identification Number:
ValueType
1959:11596Other
Keywords:Amines (N-benzylidene, redn. of)
Subjects:500 Science > 540 Chemistry & allied sciences
Status:Published
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Unknown
Owner: Petra Gürster
Deposited On:19 Nov 2010 06:37
Last Modified:19 Nov 2010 06:41
Item ID:18201
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