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[(CO)4W(PH3)2] as a source of semi-interstitial phosphorous ligands in cobalt carbonyl clusters

Dreher, Cornelia and Zabel, Manfred and Bodensteiner, Michael and Scheer, Manfred (2010) [(CO)4W(PH3)2] as a source of semi-interstitial phosphorous ligands in cobalt carbonyl clusters. Organometallics 29 (21), pp. 5187-5191.

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Other URL: http://pubs.acs.org/doi/full/10.1021/om100428p


Abstract

The PH3-containing complex [(CO)4W(PH3)2] (1) is synthesized in good yields by the “one-pot” reaction of [(CO)4W(nbd)] (nbd = norbonadiene) with P(SiMe3)3 and subsequent methanolysis of the reaction mixture. The further reaction of [(CO)4W(PH3)2] with [Co2(CO)8] results in three novel cobalt clusters, [Co8(CO)18(μ6-P)2(μ-CO)] (2), [Co10(CO)18(μ7-P)2(μ-CO)6] (3), and ...

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Item Type:Article
Date:27 July 2010
Institutions:Chemistry and Pharmacy > Institut für Anorganische Chemie > Chair Prof. Dr. Manfred Scheer
Identification Number:
ValueType
10.1021/om100428pDOI
Subjects:500 Science > 540 Chemistry & allied sciences
Status:Published
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Yes
Owner: Andreas Stauber
Deposited On:24 Feb 2011 14:07
Last Modified:24 Feb 2011 14:07
Item ID:19881
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