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Deprotection of N-alloc amines by Pd(0) /DABCO: an efficient method for in situ peptide coupling of labile amino acids

Zorn, Chiara and Gnad, Frieder and Salmen, Sunnhild and Herpin, Timothy and Reiser, Oliver (2001) Deprotection of N-alloc amines by Pd(0) /DABCO: an efficient method for in situ peptide coupling of labile amino acids. Tetrahedron Letters 42 (40), pp. 7049-7053.

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Other URL: http://dx.doi.org/10.1016/S0040-4039(01)01453-8


Abstract

A highly efficient one-pot deprotection/peptide coupling protocol of N-Alloc amino acids with activated N-Boc or N-Fmoc amino acids was developed in solution and on solid phase. DABCO was found to be especially effective for the deprotection of the N-Alloc group, resulting in short reaction times (10–20 min) and allowing the coupling of amino acids that are unstable in unprotected ...

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Item Type:Article
Date:1 October 2001
Institutions:Chemistry and Pharmacy > Institut für Organische Chemie > Lehrstuhl Prof. Dr. Oliver Reiser
Identification Number:
ValueType
10.1016/S0040-4039(01)01453-8DOI
Subjects:500 Science > 540 Chemistry & allied sciences
Status:Published
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Unknown
Owner: Helge Knüttel (ADMIN)
Deposited On:01 Sep 2006
Last Modified:05 Aug 2009 13:22
Item ID:324
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