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Optimization of Ring-Closing Metathesis: Inert Gas Sparging and Microwave Irradiation

Nosse, Bernd and Schall, Andreas and Jeong, Won Boo and Reiser, Oliver (2005) Optimization of Ring-Closing Metathesis: Inert Gas Sparging and Microwave Irradiation. Advanced Synthesis & Catalysis 347 (14), pp. 1869-1874.

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Other URL: http://dx.doi.org/10.1002/adsc.200505137


Abstract

A systematic study of a ring-closing metathesis towards a tetrasubstituted double bond as part of a seven-membered ring in a 5.7.5-tricyclic guaianolide system is described. By combining two techniques, namely sparging an inert gas through the solution together with dielectric heating via microwave irradiation a high-yielding ring-closing metathesis reaction in this particularly challenging case ...

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Item Type:Article
Date:November 2005
Institutions:Chemistry and Pharmacy > Institut für Organische Chemie > Lehrstuhl Prof. Dr. Oliver Reiser
Identification Number:
ValueType
10.1002/adsc.200505137DOI
Keywords:homogeneous catalysis; metathesis; microwave irradiation; ring-closing metathesis; ruthenium; tetrasubstituted olefin
Subjects:500 Science > 540 Chemistry & allied sciences
Status:Published
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Yes
Owner: Helge Knüttel (ADMIN)
Deposited On:05 Sep 2006
Last Modified:05 Aug 2009 13:22
Item ID:362
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