TY  - JOUR
TI  - Effects of storage and toothbrush simulation on Martens hardness of CAD/CAM, hand-cast, thermoforming, and 3D-printed splint materials
N2  - Objectives
To investigate Martens hardness parameters of splint materials after storage in liquids and toothbrush simulation.
Materials and methods
Ten specimens per material and group were fabricated (hand-cast CAST, thermoformed TF, CAD/CAM-milled CAM, 3D-printed PS, PL, PK, PV), stored in air, water, coffee, red wine, and cleaning tablets and investigated after fabrication, 24 h, 2- and 4-week storage or toothbrushing. Martens hardness (HM), indentation hardness (HIT), indentation modulus (EIT), the elastic part of indentation work (?IT), and indentation creep (CIT) were calculated (ISO 14577-1). Statistics: ANOVA, Bonferroni post hoc test, between-subjects effects, Pearson correlation (? = 0.05).
Results
HM varied between 30.8 N/mm2 for PS (water 4 weeks) and 164.0 N/mm2 for CAM (toothbrush). HIT values between 34.9 N/mm2 for PS (water 4 weeks) and 238.9 N/mm2 for CAM (toothbrush) were found. EIT varied between 4.3 kN/mm2 for CAM (toothbrush) and 1.8 kN/mm2 for PK (water 2 weeks). ?IT was found to vary between 16.9% for PS (water 4 weeks) and 42.8% for PL (toothbrush). CIT varied between 2.5% for PL (toothbrush) and 11.4% for PS (water 4 weeks). The highest impact was identified for the material (p ? 0.001).
Conclusions
Storage and toothbrushing influenced Martens parameters. The properties of splints can be influenced by the choice of materials, based on different elastic and viscoelastic parameters. High HM and EIT and low CIT might be beneficial for splint applications.
Clinical relevance
Martens parameters HM, EIT, and CIT might help to evaluate clinically relevant splint properties such as hardness, elasticity, and creep.
UR  - http://doi.org/10.1007/s00784-023-05378-4
Y1  - 2023/11/13/
A1  - Rosentritt, Martin
A1  - Hickl, Verena
A1  - Rauch, Angelika
A1  - Schmidt, Michael
PB  - Springer
SN  - 1436-3771
ID  - epub55056
KW  - Hardness · Martens · Elastic behavior · Viscoelastic parameters · Creep
AV  - public
JF  - Clinical Oral Investigations
ER  -