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Reactions of Schiff bases. V. The conversion of benzyl idenearylamines with Mg-MgI2 mixtures

Thies, Heinrich ; Schönenberger, Helmut ; Bauer, K. H.



Abstract

cf. CA 53, 3112a. Reaction of benzylidenearylamines with Mg-MgI2 mixt. proceeded faster and with better yields than that of benzylidenealkylamines. Lower yields were obtained with halogen-, MeO- or dimethylamino-substituted benzylideneanilines. A mixt. of 2.4 g. Mg and of 12.7 g. iodine in 20 ml. anhyd. Et2O and 30 ml. anhyd. C6H6 was stirred until the iodine color disappeared, 0.1 mole Schiff ...

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