Eiglsperger, A., Kastner, F. and Mannschreck, Albrecht (1985) Anwendung der NMR-Spektroskopie chiraler Assoziate 15: Flüssigkeits-Chromatographie an Triacetylcellulose 10: The enantiomers of N,N-dimethylthiobenzamides: Chromatographic behaviour and rotational barriers. Journal of Molecular Structure 126, pp. 421-432.
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Abstract
N,N-Dimethylthiobenzamides bearing hydrogen atoms in both orthopositions were shown by 1H NMR in the presence of an optically active alcohol to have non-coplanar π-systems. The barrier to rotation about the C(sp2-C(sp2) bond amounts to 43 ± 2 kJ/mol. Liquid chromatography on triacetylcellulose served for the enrichment of enantiomers of 2-substituted thiobenzamides. In several cases considerable ...
Export bibliographical data
| Item type: | Article | ||||
|---|---|---|---|---|---|
| Date: | 1985 | ||||
| Institutions: | Chemistry and Pharmacy > Institut für Organische Chemie > Alumni or Retired Professors > Prof.Dr. Mannschreck | ||||
| Identification Number: |
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| Dewey Decimal Classification: | 500 Science > 540 Chemistry & allied sciences | ||||
| Status: | Published | ||||
| Refereed: | Unknown | ||||
| Created at the University of Regensburg: | Unknown | ||||
| Item ID: | 18524 |
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