Crystal structure of 1,4-diazoniabicyclo[2.2.2]octane diiodide monohydrate

URN to cite this document:: urn:nbn:de:bvb:355-epub-258808
DOI to cite this document:: 10.5283/epub.25880

Maderlehner, Sebastian ; Pfitzner, Arno

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Date of publication of this fulltext: 14 Sep 2012 06:45

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Abstract

1,4-diazoniabicyclo [2.2.2]octane diiodide monohydrate was synthesized by protonation of 1,4-diazabicyclo[2.2.2]octane (DABCO) with an excess of concentrated hydroiodic acid in water. It forms colourless rodlike crystals. At room temperature an orthorhombic unit cell, space group Cmc2(1), a = 7.781(2) angstrom, b = 13.010(3) angstrom, c = 11.610(2) angstrom, V = 1175.3(4) angstrom(3), Z = 4, is ...