Preparation, Crystal Structure, Electronic Structure, Impedance Spectroscopy and Raman Spectroscopy of Li3SbS3 and Li3AsS3

URN to cite this document:: urn:nbn:de:bvb:355-epub-271798
DOI to cite this document:: 10.5283/epub.27179

Huber, Sebastian ; Preitschaft, Christian ; Weihrich, Richard ; Pfitzner, Arno

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Date of publication of this fulltext: 07 Jan 2013 14:21

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Abstract

Li3SbS3 was synthesized by solid-state reaction of stoichiometric amounts of Li2S and Sb2S3 in the ratio 3:1. The product is air and moisture sensitive. The crystal structure was determined from single crystals at room temperature. Pale grey Li3SbS3 crystallizes in the orthorhombic space group Pna21 (no. 33) with a = 7.9671(5) angstrom, b = 6.7883(5) angstrom, c = 10.0912(8) angstrom, V = ...