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Synthesis and (spectro)electrochemistry of mixed-valent diferrocenyl–dihydrothiopyran derivatives

URN to cite this document:
urn:nbn:de:bvb:355-epub-332976
DOI to cite this document:
10.5283/epub.33297
Kowalski, Konrad ; Karpowicz, Rafal ; Mlostoń, Grzegorz ; Miesel, Dominique ; Hildebrandt, Alexander ; Lang, Heinrich ; Czerwieniec, Rafal ; Therrien, Bruno
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Date of publication of this fulltext: 12 Feb 2016 11:10



Abstract

Three novel diferrocenyl complexes were prepared and characterised. 2,2-Diferrocenyl-4,5-dimethyl-3,6-dihydro-2H-thiopyran (1, sulphide) was accessible by the hetero-Diels–Alder reaction of diferrocenyl thioketone with 2,3-dimethyl-1,3-butadiene. Stepwise oxidation of 1 gave the respective oxides 2,2-diferrocenyl-4,5-dimethyl-3,6-dihydro-2H-thiopyran-1-oxide (2, sulfoxide) and ...

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