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Synthesis, Crystal Structure, and Physical Properties of two Polymorphs of CsGaSe2, and high temperature X-ray diffraction study of the phase transition kinetics

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Friedrich, Daniel ; Schlosser, Marc ; Pfitzner, Arno
Date of publication of this fulltext: 25 Jul 2016 13:36


The light gray selenogallate CsGaSe2-mC64 was obtained by reaction of stoichiometric amounts of CsN3, GaSe, and Se at elevated temperatures. Its crystal structure was determined by single-crystal X-ray diffraction. The compound crystallizes in the monoclinic space group C2/c (No. 15) with a = 11.043(2) Å, b = 11.015(4) Å, c = 16.810(2) Å, β = 99.49(1) °, V = 2016.7(8) Å3, and Z = 16 (powder data, ...


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