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Benzoates as photosensitization catalysts and auxiliaries in efficient, practical, light-powered direct C(sp3)–H fluorinations

Yakubov, Shahboz ; Stockerl, Willibald J. ; Tian, Xianhai ; Shahin, Ahmed ; Mandigma, Mark John P. ; Gschwind, Ruth M. ; Barham, Joshua P.



Abstract

Of the methods for direct fluorination of unactivated C(sp(3))-H bonds, photosensitization of SelectFluor is a promising approach. Although many substrates can be activated with photosensitizing catalysts, issues remain that hamper fluorination of complex molecules. Alcohol- or amine-containing functional groups are not tolerated, fluorination regioselectivity follows factors endogenous to the ...

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