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Structure Identification of Precatalytic Phosphoramidite Complexes in Solution

Zhang, H. and Gschwind, R. M. (2006) Structure Identification of Precatalytic Phosphoramidite Complexes in Solution. Angewandte Chemie International Edition 45 (38), pp. 6391-6394.

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1+1 is more than 2: A binuclear copper phosphoramidite precatalyst with mixed trigonal/tetrahedral coordination environments (see picture) is proposed based on NMR spectroscopy, mass spectrometry, and elemental analysis. The precatalyst represents a new structural motif for stereoselective copper catalysts and explains ligand acceleration and salt sensitivity in highly enantioselective 1,4-additions to enones.

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Item type:Article
Institutions:Chemistry and Pharmacy > Institut für Organische Chemie > Arbeitskreis Prof. Dr. Ruth Gschwind
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Dewey Decimal Classification:500 Science > 540 Chemistry & allied sciences
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Yes
Item ID:10631
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