Preparation and Crystal Structure of MnBiSe₂I

URN to cite this document:: urn:nbn:de:bvb:355-epub-116814
DOI to cite this document:: 10.5283/epub.11681

Pfitzner, Arno

; Zabel, Manfred ; Rau, Franz

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Date of publication of this fulltext: 23 Dec 2009 11:22

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Abstract

Black single crystals of MnBiSe2I were obtained by the reaction of stoichiometric amounts of Mn, Bi, BiI3, and Se at 600 degrees C for 7 days. The compound crystallizes in the monoclinic system, space group C2/m, with a = 13.428(2), b = 4.112(1), c = 10.130(2) angstrom, beta = 90.97(2)*, and Z = 4. The crystal structure refinement based on 849 reflections converged at R = 0.0380 and wR2 = 0.0916, ...