Preparation, Structural, Raman and Impedance Spectroscopic Characterisation of the silver ion conductor (AgI)₂Ag₃SbS₃

URN to cite this document:: urn:nbn:de:bvb:355-epub-117936
DOI to cite this document:: 10.5283/epub.11793

Nilges, Tom

; Reiser, Sara ; Hong, Jung Hoon ; Gaudin, Etienne ; Pfitzner, Arno

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Date of publication of this fulltext: 23 Dec 2009 11:38

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Abstract

Pale yellow (AgI)(2)Ag3SbS3 was synthesized by the reaction of stoichiometric amounts of AgI and Ag3SbS3 (2 : 1) at 683 K. It is air stable for several months. The crystal structure was determined at different temperatures in the range from 173 K to 573 K by single crystal X-ray diffraction. (AgI)(2)Ag3SbS3 crystallizes in the orthorhombic system, space group Pnnm (no. 58) with a = 10.9674(8) ...