Preparation and Crystal Structure of MnBiS₂Br

URN to cite this document:: urn:nbn:de:bvb:355-epub-118367
DOI to cite this document:: 10.5283/epub.11836

Pfitzner, Arno

; Zabel, Manfred ; Rau, Franz

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Date of publication of this fulltext: 23 Dec 2009 11:41

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Abstract

Black single crystals of MnBiS2Br were obtained by the reaction of stoichiometric amounts of alpha-MnS, Bi, S, and BiBr3 (3:2:3:1) at 600 degrees C for 4 weeks. The compound crystallises in the monoclinic system, space group C2/m, with a = 12.767(2), b = 3.9468(4), c = 9.574(1) A, beta = 90.87(2)degrees, and Z = 4. The crystal structure refinement based on 720 reflections converged at R = 0.0244 ...