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Synthesis and luminescence properties of cyclometallated platinum complexes with substituted thienylpyridines

Kozhevnikov, V. N. ; Kozhevnikov, D. N. ; Ustinova, M. M. ; Bruce, D. W. ; Koenig, B. ; Czerwieniec, R. ; Fischer, T. ; Yersin, Hartmut



Abstract

Synthesis of various derivatives of 2-(2-thienyl)pyridine via substituted 3-thienyl-1,2,4-triazines is reported. The final step of the synthesis is a transformation of the triazine ring to pyridine in an aza-Diels-Alder-type reaction. The resulting 5-aryl-2-(2-thienyl)pyridines (HL1-HL4) and 5-aryl 2-(2-thienyl)cyclopenteno[c]pyridines (HL5-HL8) (with aryl = phenyl, 4-methoxyphenyl, 2-naphtyl, ...

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