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Separation of organic bases by Craig partition. VI. Correlations between the configuration and the phase distribution behavior of aminoacylephedrines

Schönenberger, Helmut ; Brinkmann, Rolf



Abstract

cf. CA 62, 7857h. A series of diastereomeric aminoacylephedrine compds. were sepd. in a Craig phase distribution process in a mixt. of CHCl3, MeOH, and citrate buffer soln. (vol. 10:1:9) at 20 Deg (distribution coeff., K, and sepn. factor, beta = K2/KD, given): (L-N-dimethylphenylalanyl)-L-amphetamine, 1.1, (D-N-dimethylphenylalanyl)-L-amphetamine, 0.75, 1.4; ...

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