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Cystostatic agents. III. Mechanism of reduction of Schiff bases by activated aluminum

Schönenberger, Helmut, Thies, Heinrich and Rappl, A. (1965) Cystostatic agents. III. Mechanism of reduction of Schiff bases by activated aluminum. Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft 298 (6), pp. 367-371.

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cf. Schoenenberger, et al., CA 62, 6992f, 7664a, 13163g. The mechanism of redn. was investigated of benzylidenealkyl- and benzylidenearylamine-type Schiff bases with activated Al, to form mono- and dimeric secondary amines. Redn. of PhCH:NBu (I) in abs. EtOH with Al-Hg gave yields of benzylbutylamine (II) and N,N'-dibutyl-alpha ,alpha '-diphenylethylenediamine (III) (in meso- and racemic forms) ...


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Item type:Article
Additional Information (public):CAN 63:31027 32 Physical Organic Chemistry 2403-22-7P (Benzylamine, N-butyl-) Role: PREP (Preparation) (formation from N-benzylidenebutylamine and isopropylmagnesium halides, in N-benzylidenebutylamine redn. with Al-Hg); 544-40-1 (Butyl sulfide) (hydrogenolysis of, solvent effect in); 1165-52-2P (Ethylenediamine, N,N'-dibutyl-1,2-diphenyl-, meso-); 4169-62-4P (Ethylenediamine, N,N'-dibutyl-1,2-diphenyl-, (-)-) Role: PREP (Preparation) (prepn. of); 1077-18-5 (Butylamine, N-benzylidene-) (redn. of, by Al-Hg); 7439-97-6 (Mercury) (N-benzylidenebutylamine redn. by Al and); 7429-90-5 (Aluminum) (N-benzylidenebutylamine redn. by Hg and)
Institutions:Chemistry and Pharmacy > Institute of Pharmacy > Alumni or Retired Professors > Prof. Schönenberger
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Dewey Decimal Classification:500 Science > 540 Chemistry & allied sciences
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Unknown
Item ID:18187
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