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Reduction of benzylidene alkylamines with activated aluminum in alcoholic solution

Thies, Heinrich ; Schönenberger, Helmut ; Bauer, K. H.


Dialkyldiphenylethylenediamines and benzylalkylamines were formed on reduction of benzylidenealkylamines with activated Al. Al foil (5.4 g.) and a little HgCl2. in 120 ml. EtOH warmed until H began to evolve, 0.1 mole Schiff base in 30 ml. C6H6 added, the mixt. heated 2 hrs. on the H2O bath, treated with 100 ml. C6H6 and 100 ml. 15% aq. NaOH, heated 15 min. more, 200 ml. H2O added, the mixt. ...


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