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Dimerization of piperidinoacetonitrile under the influence of Grignard reagents

Thies, H. ; Schönenberger, Helmut ; Qasba, P. K.


The reaction of piperidinoacetonitrile with tert-BuMgCl leads to 3-amino-2,4-dipiperidinocrotononitrile (I), b0.3 167 Deg, m. 86-7 Deg iso-(PrOH) (Thompson, CA 53, 8155f). The infrared spectrum of I is discussed.

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