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Reactions of alpha -aminonitriles. VII. Dimer exchange products of aromatic substituted aminonitriles

Thies, Heinrich, Schönenberger, Helmut and Qasba, P. K. (1969) Reactions of alpha -aminonitriles. VII. Dimer exchange products of aromatic substituted aminonitriles. Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft 302 (11), pp. 803-807.

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The reaction of Et2NCHPhCN with Na in PhMe gave 39.2% Et2NCH2Ph, b16 85-7 Deg, and 44.6% Et2NCHPhCHPhNEt2 b0.4 140 Deg. Similarly prepd. were 38.7% Et2NCH2C6H4OMe-p, b15 126 Deg and 52.2% I, b0.3 180-6 Deg. The dimers could not be purified. In the open air I gave p,p'-deoxyanisoin. The compn. and spectral detn. of the impurities are discussed.

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Item type:Article
Additional Information (public):CAN 72:42998 25 Noncondensed Aromatic Compounds 108-88-3 Role: USES (Uses) (amino nitrile reaction with sodium in presence of); 120-44-5P; 772-54-3P; 800-13-5P; 24932-53-4P; 24932-54-5P Role: SPN (Synthetic preparation), PREP (Preparation) (prepn. of); 7440-23-5 Role: RCT (Reactant), RACT (Reactant or reagent) (with amino nitriles in presence of toluene)
Institutions:Chemistry and Pharmacy > Institute of Pharmacy > Alumni or Retired Professors > Prof. Schönenberger
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Keywords:Nitriles Role: RCT (Reactant), RACT (Reactant or reagent) (alpha -amino, with sodium in presence of toluene) nitriles amino dimerization amino nitriles dimerization benzyl amines dimers dimers amines benzyl
Dewey Decimal Classification:500 Science > 540 Chemistry & allied sciences
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Unknown
Item ID:18210
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