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Chiroptical Detection after Liquid Chromatography 2: Enantiomerization during HPLC on an optically active sorbent. Deconvolution of experimental chromatograms

Mannschreck, Albrecht ; Kießl, L.


The enantiomers of 1,3,7-trimethylbenzo[c]phenanthrene, a chiral helicene hydrocarbon, are separated on triacetyl-cellulose but interconvert during HPLC. Column temperatures were between 2 and 22°C and linear velocities between 0.3 and 1.2 mm s–1. Simultaneous photometric and polarimetric detection resulted in deconvoluted experimental chromatograms, showing the relative concentration of each of ...


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