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What is your actual catalyst? TMS cleavage rates of diarylprolinol silyl ethers studied by in situ NMR

Haindl, Michael H., Schmid, Markus Benedikt, Zeitler, Kirsten and Gschwind, Ruth Maria (2012) What is your actual catalyst? TMS cleavage rates of diarylprolinol silyl ethers studied by in situ NMR. RSC Advances 2, pp. 5941-5943.

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Other URL: http://dx.doi.org/10.1039/C2RA20860A


Abstract

Diarylprolinol silyl ethers are excellent and broadly applicable organocatalysts for various enamine and iminium-type synthetic transformations. However, their undesired degradation to the corresponding diarylprolinols and the subsequent formation of oxazolidines during reaction with aldehydes may significantly affect their catalytic performance. Therefore, in situ NMR was used to examine the TMS ...

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Item type:Article
Date:2012
Institutions:Chemistry and Pharmacy > Institut für Organische Chemie > Arbeitskreis Prof. Dr. Ruth Gschwind
Identification Number:
ValueType
10.1039/C2RA20860ADOI
Dewey Decimal Classification:500 Science > 540 Chemistry & allied sciences
Status:Published
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Yes
Item ID:26490
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