Na3SbSe3: Synthesis, Crystal Structure Determination, Raman-Spectroscopy, and Ionic Conductivity

URN to cite this document:: urn:nbn:de:bvb:355-epub-265603
DOI to cite this document:: 10.5283/epub.26560

Pompe, Constantin

; Pfitzner, Arno

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Date of publication of this fulltext: 26 Oct 2012 08:58

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Abstract

Na3SbSe3 was obtained by solid state reaction of anhydrous Na2Se, antimony, and selenium in a ratio of 3:2:3. It is air and moisture sensitive and melts at 870 K. Yellow single crystals of Na3SbSe3 were used for single-crystal X-ray diffraction. It crystallizes in the cubic space group P213 (No. 198) with a = 9.0227(2) angstrom, V = 734.53(3) angstrom 3, and Z = 4. Na3SbS3 is isotypic with ...