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Synthesis and crystal structure determination of Ag9FeS4.1Te1.9, the first example of an iron containing argyrodite

URN to cite this document:
Frank, D. ; Gerke, B. ; Eul, M. ; Pöttgen, R. ; Pfitzner, Arno
Date of publication of this fulltext: 31 May 2013 10:57


Ag9FeS4.1Te1.9 was prepared by solid state synthesis from stoichiometric amounts of the elements at 873 K. The compound forms grey crystals which are stable against air and moisture. The crystal structure was determined by X-ray diffraction from selected single crystals. Ag9FeS4.1Te1.9 crystallizes in the space group F4¯3m, a = 11.0415(7) Å, V = 1346.1(1) Å3, and Z = 4 (powder data at 293 K). The ...


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