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Asymmetric Synthesis of both Enantiomers of Arteludovicinolide A

Kreuzer, A. ; Kerres, S. ; Ertl, T. ; Rücker, Hannelore ; Amslinger, S. ; Reiser, Oliver


The first total synthesis of either enantiomer of Arteludovicinolide A and their biological evaluation is reported, featuring a new strategy for the asymmetric construction of γ-butyrolactones with stereogenic side chains in the 4-position. Starting from the renewable resource methyl 2-furoate, the sesquiterpene lactone was synthesized in 9 steps and 4.8% overall yield via an asymmetric ...


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