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Flux synthesis and crystal structure determination of the colored skutterudite Ir2Sn3Se3

Yan, W. ; Pielnhofer, F. ; Tragl, A. S. ; Weihrich, Richard



Abstract

The skutterudite (CoSb3) related crystal structure of Ir2Sn3Se3 = IrSn1.5Se1.5 is determined from single crystal data for the first time. High temperature solid state and flux reactions were applied to prepare powder and single crystals samples. Its crystal structure was refined from data of a fourfold twin crystal in space group R (3) over bar (no. 148). It contains 24 formula units per unit ...

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