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In-situ investigation of two-step nucleation and growth of CdS nanoparticles from solution

Schiener, A. ; Magerl, A. ; Krach, A. ; Seifert, S. ; Steinrück, H. G. ; Zagorac, J. ; Zahn, D. ; Weihrich, Richard


We report on a combined ultra-fast in situ SAXS and WAXS study along a free-jet providing insight into the evolution of the morphology and crystalline structure of CdS quantum dots in the very early stage of nucleation between 100 μs and 2.5 ms with a time resolution down to 10 μs. Accessing this yet unexplored time regime provides direct evidence of a two-step mechanism via formation of ...


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