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The approach to 4d/4f-polyphosphides

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Arleth, Nicholas ; Gamer, Michael T. ; Köppe, Ralf ; Pushkarevsky, Nikolay A. ; Konchenko, Sergey N. ; Fleischmann, Martin ; Bodensteiner, Michael ; Scheer, Manfred ; Roesky, Peter W.
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Date of publication of this fulltext: 16 Feb 2016 09:58


The first 4d/4f polyphosphides were obtained by reaction of the divalent metallocenes [Cp*2Ln(thf)2] (Ln = Sm, Yb) with [{CpMo(CO)2}2(μ,η2:2-P2)] or [Cp*Mo(CO)2(η3-P3)]. Treatment of [Cp*2Ln(thf)2] (Ln = Sm, Yb) with [{CpMo(CO)2}2(μ,η2:2-P2)] gave the 16-membered bicyclic compounds [(Cp2*Ln)2P2(CpMo(CO)2)4] (Ln = Sm, Yb) as the major products. From the reaction involving samarocene, the cyclic P4 ...


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