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Intramolecular monomer-on-monomer (MoM) Mitsunobu cyclization for the synthesis of benzofused thiadiazepine-dioxides

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Maity, P. ; Kainz, Quirin ; Faisal, Saqib ; Rolfe, Alan ; Samarakoon, T. ; Basha, F. ; Reiser, Oliver ; Hanson, P.
License: Allianz- bzw. Nationallizenz
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Date of publication of this fulltext: 26 Jul 2016 11:01


The utilization of a monomer-on-monomer (MoM) intramolecular Mitsunobu cyclization reaction employing norbornenyl-tagged (Nb-tagged) reagents is reported for the synthesis of benzofused thiadiazepine-dioxides. Facile purification was achieved viaring-opening metathesis (ROM) polymerization initiated by one of three metathesis catalyst methods: (i) free metathesis catalyst, (ii) surface-initiated catalyst-armed silica, or (iii) surface-initiated catalyst-armed Co/C magnetic nanoparticles.

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