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Maity, P. ; Kainz, Quirin ; Faisal, Saqib ; Rolfe, Alan ; Samarakoon, T. ; Basha, F. ; Reiser, Oliver ; Hanson, P.

Intramolecular monomer-on-monomer (MoM) Mitsunobu cyclization for the synthesis of benzofused thiadiazepine-dioxides

Maity, P., Kainz, Quirin, Faisal, Saqib, Rolfe, Alan, Samarakoon, T., Basha, F., Reiser, Oliver and Hanson, P. (2011) Intramolecular monomer-on-monomer (MoM) Mitsunobu cyclization for the synthesis of benzofused thiadiazepine-dioxides. Chemical Communications (47), pp. 12524-2526.

Date of publication of this fulltext: 26 Jul 2016 11:01
Article
DOI to cite this document: 10.5283/epub.34148


Abstract

The utilization of a monomer-on-monomer (MoM) intramolecular Mitsunobu cyclization reaction employing norbornenyl-tagged (Nb-tagged) reagents is reported for the synthesis of benzofused thiadiazepine-dioxides. Facile purification was achieved viaring-opening metathesis (ROM) polymerization initiated by one of three metathesis catalyst methods: (i) free metathesis catalyst, (ii) surface-initiated catalyst-armed silica, or (iii) surface-initiated catalyst-armed Co/C magnetic nanoparticles.



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Details

Item typeArticle
Journal or Publication TitleChemical Communications
Publisher:Royal Society of Chemistry
Number of Issue or Book Chapter:47
Page Range:pp. 12524-2526
Date2011
InstitutionsChemistry and Pharmacy > Institut für Organische Chemie > Lehrstuhl Prof. Dr. Oliver Reiser
Identification Number
ValueType
10.1039/C1CC14807ADOI
Dewey Decimal Classification500 Science > 540 Chemistry & allied sciences
StatusPublished
RefereedYes, this version has been refereed
Created at the University of RegensburgYes
URN of the UB Regensburgurn:nbn:de:bvb:355-epub-341480
Item ID34148

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