Study of the mechanochemical process to crystalline Cu2ZnSnS4 powder

URN to cite this document:: urn:nbn:de:bvb:355-epub-345778
DOI to cite this document:: 10.5283/epub.34577

Ritscher, A. ; Schlosser, Marc

; Pfitzner, Arno

; Lerch, M.

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Date of publication of this fulltext: 13 Sep 2016 11:24

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Abstract

Kesterite-type Cu2ZnSnS4 was synthesized from the corresponding binary sulfides by a mechanochemical route in a planetary ball mill. The reaction progress during this milling step was followed within a time range of 10-180 min by powder X-ray diffraction. In addition, the crystallization of the milled material was studied in situ by high-temperature X-ray diffraction methods in the temperature ...