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Study of the mechanochemical process to crystalline Cu2ZnSnS4 powder
Ritscher, A., Schlosser, Marc
, Pfitzner, Arno und Lerch, M.
(2016)
Study of the mechanochemical process to crystalline Cu2ZnSnS4 powder.
Materials Research Bulletin 84, S. 162-167.
Veröffentlichungsdatum dieses Volltextes: 13 Sep 2016 11:24
Artikel
DOI zum Zitieren dieses Dokuments: 10.5283/epub.34577
Zusammenfassung
Kesterite-type Cu2ZnSnS4 was synthesized from the corresponding binary sulfides by a mechanochemical route in a planetary ball mill. The reaction progress during this milling step was followed within a time range of 10-180 min by powder X-ray diffraction. In addition, the crystallization of the milled material was studied in situ by high-temperature X-ray diffraction methods in the temperature ...
Kesterite-type Cu2ZnSnS4 was synthesized from the corresponding binary sulfides by a mechanochemical route in a planetary ball mill. The reaction progress during this milling step was followed within a time range of 10-180 min by powder X-ray diffraction. In addition, the crystallization of the milled material was studied in situ by high-temperature X-ray diffraction methods in the temperature range of 300500 degrees C. Significant disorder (cation distribution) was observed at 500 degrees C, strongly decreasing during cooling down to ambient temperature with a rate of 60K/h. (C) 2016 Elsevier Ltd. All rights reserved.
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| Dokumentenart | Artikel | ||||
| Titel eines Journals oder einer Zeitschrift | Materials Research Bulletin | ||||
| Verlag: | PERGAMON-ELSEVIER SCIENCE LTD | ||||
|---|---|---|---|---|---|
| Ort der Veröffentlichung: | OXFORD | ||||
| Band: | 84 | ||||
| Seitenbereich: | S. 162-167 | ||||
| Datum | 2016 | ||||
| Institutionen | Chemie und Pharmazie > Institut für Anorganische Chemie > Lehrstuhl Prof. Dr. Arno Pfitzner | ||||
| Identifikationsnummer |
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| Stichwörter / Keywords | KESTERITE; TRANSITION; ABSORBER; Semiconductors; Chemical synthesis; X-ray diffraction; Crystal structure; Defects | ||||
| Dewey-Dezimal-Klassifikation | 500 Naturwissenschaften und Mathematik > 540 Chemie | ||||
| Status | Veröffentlicht | ||||
| Begutachtet | Ja, diese Version wurde begutachtet | ||||
| An der Universität Regensburg entstanden | Ja | ||||
| URN der UB Regensburg | urn:nbn:de:bvb:355-epub-345778 | ||||
| Dokumenten-ID | 34577 |
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