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Study of the mechanochemical process to crystalline Cu2ZnSnS4 powder
Ritscher, A., Schlosser, Marc
, Pfitzner, Arno and Lerch, M.
(2016)
Study of the mechanochemical process to crystalline Cu2ZnSnS4 powder.
Materials Research Bulletin 84, pp. 162-167.
Date of publication of this fulltext: 13 Sep 2016 11:24
Article
DOI to cite this document: 10.5283/epub.34577
Abstract
Kesterite-type Cu2ZnSnS4 was synthesized from the corresponding binary sulfides by a mechanochemical route in a planetary ball mill. The reaction progress during this milling step was followed within a time range of 10-180 min by powder X-ray diffraction. In addition, the crystallization of the milled material was studied in situ by high-temperature X-ray diffraction methods in the temperature ...
Kesterite-type Cu2ZnSnS4 was synthesized from the corresponding binary sulfides by a mechanochemical route in a planetary ball mill. The reaction progress during this milling step was followed within a time range of 10-180 min by powder X-ray diffraction. In addition, the crystallization of the milled material was studied in situ by high-temperature X-ray diffraction methods in the temperature range of 300500 degrees C. Significant disorder (cation distribution) was observed at 500 degrees C, strongly decreasing during cooling down to ambient temperature with a rate of 60K/h. (C) 2016 Elsevier Ltd. All rights reserved.
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| Item type | Article | ||||
| Journal or Publication Title | Materials Research Bulletin | ||||
| Publisher: | PERGAMON-ELSEVIER SCIENCE LTD | ||||
|---|---|---|---|---|---|
| Place of Publication: | OXFORD | ||||
| Volume: | 84 | ||||
| Page Range: | pp. 162-167 | ||||
| Date | 2016 | ||||
| Institutions | Chemistry and Pharmacy > Institut für Anorganische Chemie > Chair Prof. Dr. Arno Pfitzner | ||||
| Identification Number |
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| Keywords | KESTERITE; TRANSITION; ABSORBER; Semiconductors; Chemical synthesis; X-ray diffraction; Crystal structure; Defects | ||||
| Dewey Decimal Classification | 500 Science > 540 Chemistry & allied sciences | ||||
| Status | Published | ||||
| Refereed | Yes, this version has been refereed | ||||
| Created at the University of Regensburg | Yes | ||||
| URN of the UB Regensburg | urn:nbn:de:bvb:355-epub-345778 | ||||
| Item ID | 34577 |
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