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1,10-Phenanthroline-dithiine iridium and ruthenium complexes: synthesis, characterization and photocatalytic dihydrogen evolution

Erdmann, Elisa ; Villinger, A. ; König, Burkhard ; Seidel, W. W.


We report the synthesis and the spectroscopic and electrochemical properties of six mononuclear iridium(iii) and ruthenium(ii) complexes bearing S,S-extended phenanthroline ligands. Starting from 5,6-dibromide-1,10-phenanthroline, the dithiine derivatives N,N-1,10-phenanthrolinedithiino[2,3-b]quinoxaline and N,N-1,10-phenanthrolinedithiino[2,3-b]benzene were prepared by primary N,N-complexation ...


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