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Aromatic Chlorosulfonylation by Photoredox Catalysis

Májek, Michal, Neumeier, Michael and Jacobi von Wangelin, Axel (2016) Aromatic Chlorosulfonylation by Photoredox Catalysis. ChemSusChem 10 (1), pp. 151-155.

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Other URL: http://doi.org/10.1002/cssc.201601293


Visible-light photoredox catalysis enables the efficient synthesis of arenesulfonyl chlorides from anilines. The new protocol involves the convenient in situ preparation of arenediazonium salts (from anilines) and the reactive gases SO2 and HCl (from aqueous SOCl2). The photocatalytic chlorosulfonylation operates at mild conditions (room temperature, acetonitrile/water) with low catalyst loading. ...


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Item type:Article
Institutions:Chemistry and Pharmacy > Institut für Organische Chemie > Arbeitskreis Prof. Dr. Axel Jacobi von Wangelin
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Keywords:SULFONYL CHLORIDES; METAL-FREE; SULFUR-DIOXIDE; SALTS; ALKYL; ARYLATION; ANILINES; aromatic substitution; photochemistry; photoredox catalysis; ruthenium; sulfonylation
Dewey Decimal Classification:500 Science > 540 Chemistry & allied sciences
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Yes
Item ID:38811
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