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Development and Application of a Recyclable High-Load Magnetic Co/C Hybrid ROMP-Derived Benzenesulfonyl Chloride Reagent and Utility of Corresponding Analogues

Faisal, Saqib, Zang, Qin, Maity, Pradip K., Brandhofer, Agnes, Kearney, Patrick C., Reiser, Oliver , Grass, Robert N., Stoianova, Diana and Hanson, Paul R. (2017) Development and Application of a Recyclable High-Load Magnetic Co/C Hybrid ROMP-Derived Benzenesulfonyl Chloride Reagent and Utility of Corresponding Analogues. Organic Letters 19 (9), pp. 2274-2277.

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Other URL: http://doi.org/10.1021/acs.orglett.7b00792


Abstract

The development and application of high-load, recyclable magnetic Co/C hybrid ROMP-derived benzenesulfonyl chloride and analogues is reported. The regeneration and utility of these reagents in the methylation/alkylation of various carboxylic acids is demonstrated via efficient retrieval of the magnetic reagent with a neodymium magnet. Additional reactions employing the analogue sulfonic acid and in situ generated magnetic benzenesulfonyl azide are also reported.


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Item type:Article
Date:2017
Institutions:Chemistry and Pharmacy > Institut für Organische Chemie > Lehrstuhl Prof. Dr. Oliver Reiser
Identification Number:
ValueType
10.1021/acs.orglett.7b00792DOI
Keywords:CARBOXYLIC-ACIDS; METATHESIS POLYMERIZATION; ALKYLATING REAGENTS; DIAZODICARBONYL COMPOUNDS; CONTINUOUS-FLOW; ONE-POT; EFFICIENT; ESTERIFICATION; CATALYSTS; NANOPARTICLES;
Dewey Decimal Classification:500 Science > 540 Chemistry & allied sciences
Status:Published
Refereed:Yes, this version has been refereed
Created at the University of Regensburg:Yes
Item ID:39006
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