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Synthesis and Characterization of the High-Pressure Nickel Borate γ-NiB4O7

Schmitt, Martin K. ; Janka, Oliver ; Niehaus, Oliver ; Dresselhaus, Thomas ; Pöttgen, Rainer ; Pielnhofer, Florian ; Weihrich, Richard ; Krzhizhanovskaya, Maria ; Filatov, Stanislav ; Bubnova, Rimma ; Bayarjargal, Lkhamsuren ; Winkler, Björn ; Glaum, Robert ; Huppertz, Hubert



Abstract

gamma-NiB4O7 was synthesized in a high-pressure/high-temperature experiment at 5 GPa and 900 degrees C. The, single-crystal structure analysis yielded the following, results: space group P6(5)22 (No. 179), a = 425.6(2), c = 3490.5(2) pm, V = 0.545(2). nm(3), Z = 6, and Flack parameter x = -0.010(5). Second harmonic generation Measurements confirmed the acentric crystal structure. Furthermore, ...

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