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Bis-cyclometalated rhodium- and iridium-complexes with the 4,4′-dichloro-2,2′-bipyridine ligand. Evaluation of their photophysical properties and biological activity

Graf, Marion ; Gothe, Yvonne ; Metzler-Nolte, Nils ; Czerwieniec, Rafał ; Sünkel, Karlheinz


The synthesis and characterization of new cyclometalated complex salts [M(C boolean AND N)(2)(4,4',-Cl(2)bpy)]PF6 (M = Rh and Ir; CAN = 2-(p-tolyl)pyridinato (1 and 2), 2-phenyl-5-chloro-pyridinato (3 and 4); 4,4'-Cl(2)bpy = 4,4'-dichloro-2,2'-bipyridine) is described. Compounds 1-4 were obtained by reaction of 4,4'dichloro-2,2'-bipyridine with the complexes [{M(mu-Cl)(C boolean AND N)(2)}(2)] (M ...


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