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Oxidative photochlorination of electron rich arenes via in situ bromination

Düsel, Simon J. S. ; König, Burkhard



Abstract

Electron rich arenes are oxidatively photochlorinated in the presence of catalytic amounts of bromide ions, visible‐light and 4CzIPN as organic photoredox catalyst. The substrates are in situ brominated in a first photoredox‐catalyzed oxidation step, followed by a photocatalyzed ipso‐chlorination yielding the target compounds in high ortho/para regioselectivity. Dioxygen serves as a green and ...

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