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Synthesis and Characterization of Naphtho[2,1‐b:7,8‐b′]bis[1]benzothiophene

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Kaiser, Jens ; Mekic, Amel ; Parham, Amir Hossain ; Buchholz, Herwig ; König, Burkhard
License: Creative Commons: Attribution 3.0
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Date of publication of this fulltext: 18 Feb 2020 12:22

This publication is part of the DEAL contract with Wiley.


We describe a simple three‐step synthesis of naphtho[2,1‐b:7,8‐b′]bis[1]benzothiophene, which is scalable to multi‐hundred‐gram. We report the subsequent functionalization of this compound into iodine, boronic ester and silane derivatives, which are useful intermediates for various applications. The core structure was analyzed by NMR and single‐crystal X‐ray diffraction, and the physical properties were investigated by cyclic voltammetry, UV/Vis‐ and fluorescence spectroscopy.

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