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Transfer Hydrogenation of Azo Compounds with Ammonia Borane Using a Simple Acyclic Phosphite Precatalyst

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Chacón‐Terán, M. A. ; Rodríguez‐Lugo, R. E. ; Wolf, Robert ; Landaeta, V. R.
License: Creative Commons: Attribution-Noncommercial 3.0
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Date of publication of this fulltext: 20 Feb 2020 12:55

This publication is part of the DEAL contract with Wiley.


Tris(quinolin-8-yl)phosphite, P(Oquin)(3), promotes the dehydrogenation of H3N center dot BH3 (AB) and the transfer hydrogenation of azoarenes using ammonia borane (AB) as H-2 source. The metal-free reduction of azoarenes proceeds under mild reaction conditions upon which several diphenylhydrazine derivatives are obtained in high yields. The reactivity of P(Oquin)(3) toward AB was evaluated ...


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