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Methods for the comprehensive structural elucidation of constitution and stereochemistry of lipopeptides

Gerhardt, Heike ; Sievers-Engler, Adrian ; Jahanshah, Ghazaleh ; Pataj, Zoltán ; Ianni, Federica ; Gross, Harald ; Lindner, Wolfgang ; Lämmerhofer, Michael


A panel of methods of general suitability for complete structural elucidation of the stereochemistry of cyclopeptides, depsipeptides and lipopeptides is presented and described in detail. The suitability of the proposed methods was exemplified on the lipopeptide poaeamide from Pseudomonas poae. Amino acid configurations have been assigned by direct LC enantiomer separation with Chiralpak ZWIX(+) ...


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