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Room-Temperature Synthesis of Thiostannates from {[Ni(tren)]2[Sn2S6]}n

Hilbert, Jessica ; Näther, Christian ; Weihrich, Richard ; Bensch, Wolfgang


The compound {[Ni(tren)](2)[Sn2S6]}(n) (1) (tren = tris(2-aminoethyl)amine, C6H18N4) was successfully applied as source for the room-temperature synthesis of the new thiostannates [Ni(tren)(ma)(H2O)](2)[Sn2S6]center dot 4H(2)O (2) (ma = methylamine, CH5N) and [Ni(tren)(1,2-dap)](2)[(SnS6)-S-2]center dot 2H(2)O (3) (1,2-dap = 1,2-diaminopropane, C3H10N2). The Ni-S bonds in the Ni2S2N8 bioctahedron ...


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