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Synthesis, Crystal Structure, and Physical Properties of Two Polymorphs of CsGaSe2, and High-Temperature X-ray Diffraction Study of the Phase Transition Kinetics

Friedrich, Daniel ; Schlosser, Marc ; Pfitzner, Arno



Abstract

The light gray selenogallate CsGaSe2-mC64 was obtained by reaction of stoichiometric amounts of CsN3, GaSe, and Se at elevated temperatures. Its crystal structure was determined by single-crystal X-ray diffraction. The compound crystallizes in the monoclinic space group C2/c (No. 15) with a = 11.043(2) angstrom, b = 11.015(4) angstrom, c= 16.810(2) angstrom, beta = 99.49(1)degrees, v = 2016.7(8) ...

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