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Regioselective Thiocarbonylation of Vinyl Arenes

Hirschbeck, Vera ; Gehrtz, Paul H. ; Fleischer, Ivana


A palladium-catalyzed thiocarbonylation of styrene derivatives is reported for the first time. The combination of thiols as nucleophiles and a bidentate ligand ensures a unique reaction outcome with high regioselectivity toward the more valuable branched isomer and new reactivity. The ambient reaction conditions (temperature, catalyst loading) and the use of a CO surrogate render this ...


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