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Co-Crystallization of Half-Sandwich (R M ,R C )/(S M ,R C ) Diastereomers in Single Crystals

Brunner, Henri ; Tsuno, Takashi ; Bodensteiner, Michael ; Gärtner, Stefanie ; Miyahara, Chiemi ; Ito, Seera ; Kurosawa, Takaki ; Koyama, Kazuhiro



Abstract

Diastereomer separation by fractional crystallization is the most important method for the resolution of enantiomers in research as well as in industry. Herein we describe two different types of diastereomer co-crystallization, which impede diastereomer separation. The two diastereomers (R-Fe,R-C)- and (S-Fe,R-C)-[CpFe(Prophos)PPh(OMe)(2)]PF6, differing only in the metal atom configuration, form ...

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