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C(sp3)−C(sp3) Cross‐Coupling of Alkyl Bromides and Ethers Mediated by Metal and Visible Light Photoredox Catalysis

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Santos, Marilia S. ; Corrêa, Arlene G. ; Paixão, Márcio W. ; König, Burkhard
License: Creative Commons Attribution 4.0
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Date of publication of this fulltext: 08 May 2020 06:00

This publication is part of the DEAL contract with Wiley.


We report a C(sp(3))-C(sp(3)) cross-coupling of alkyl bromides and alkyl chlorides with ethers by dual photoredox-nickel catalysis. The catalytic system comprises of the organic photocatalyst 1,2,3,5-tetrakis(carbazol-9-yl)-4,6-dicyanobenzene (4-CzIPN) and bench stable nickel (II) acetylacetonate in the presence of visible-light, providing the coupling products in up to 92% yield. Preliminary ...


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