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Expedient Hydrofunctionalisation of Carbonyls and Imines Initiated by Phosphacyclohexadienyl Anions

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Margeson, Matthew J. ; Seeberger, Felix ; Kelly, John A. ; Leitl, Julia ; Coburger, Peter ; Szlosek, Robert ; Müller, Christian ; Wolf, Robert
License: Creative Commons Attribution Non-commercial 4.0
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Date of publication of this fulltext: 22 Jun 2021 06:08

This publication is part of the DEAL contract with Wiley.


The ability of phosphacyclohexadienyl anions [Li(1-R-PC5Ph3H2)] [R=Me (1 a), nBu (1 b), tBu (1 c), Ph (1 d) and CH2SiMe3 (1 e)] to initiate hydrofunctionalisation reactions was investigated and compared with simple, commercially available compounds, such as LiOtBu, KOtBu and nBuLi. All compounds are expedient catalysts for the hydroboration of a wide scope of substrates, ranging from aldehydes to ...


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