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Selective Synthesis and Thermodynamic Relations of Polymorphic Co(NCS)2 -4-Dimethylaminopyridine Coordination Compounds

Neumann, Tristan ; Jess, Inke ; Pielnhofer, Florian ; Näther, Christian



Abstract

Reaction of Co(NCS)(2) with 4-dimethylaminopyridine (DMAP) leads to the formation of four new compounds. The crystal structures of Co(NCS)(2)(DMAP)(2)(H2O)(2)center dot 2H(2)O (1), Co(NCS)(2)(DMAP)(2)(MeOH)(2) (2) and Co(NCS)(2)(DMAP)(2)(MeCN)(2) (3) consist of discrete simple solvato complexes in which the Co cations are octahedrally coordinated by two terminally N-bonded thiocyanate anions, two ...

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