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Synthesis and Characterization of Cs 4 Ga 6 Q 11 (Q=S, Se): Chalcogenometalates with Exotic Polymeric Anions

Friedrich, Daniel ; Greim, Dominik ; Schlosser, Marc ; Siegel, Renée ; Senker, Jürgen ; Pfitzner, Arno


Two new chalcogenogallates Cs(4)Ga(6)Q(11) (Q = S, Se) were obtained by a controlled thermal treatment of CsN3 in the presence of stoichiometric amounts of Ga(2)Q(3) and the elemental chalcogens at elevates temperatures. Both isotypic compounds crystallize in the space group P (1) over bar (no. 2). The most prominent structural feature in these chalcogenogallates are the complex anionic Dreier ...


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